ICP-OES
  • ICP-OES

    • DW-ICP-OES3000 Inductively Coupled Plasma Optical Emission Spectrometer

    DW-ICP-OES3000 inductively coupled plasma emission spectrometer is a powerful performance, simultaneous full-spectrum direct-reading spectrometer developed by Drawell, which is used for trace elemental analysis in diverse samples (soluble in hydrochloric acid, nitric acid, hydrofluoric acid. etc). The instrument offers capabilities with automatization, stability, reliability, and ease of use. It is currently widely applied in various fields of rare earth, geological, metallurgical, chemical, environmental, clinical medicine, petroleum, semiconductor, food, biological samples, criminal science, agricultural research, etc…

    DW-ICP-OES3000 Manual
    DW-ICP-OES3000 Brochure

    Application Fields

    • Silicon Industrial: magnetic materials
    • Metallurgical: analyze As, Bi, Pb, Sb, Sn, and other impurity elements, which affect greatly the quality of the metallic materials
    • Water analysis: analyze 8 heavy metal elements
    • Geological, minera: analyze Ca, Mg, Na, Fe, Cu, Mn, Zn, Co, Ni, Au, Ag, and other elements in the rock samples
    • Petrochemical and Industrial: Analyze over 30 elements in crude oil, mainly Fe, Na, Mg, Ni, V, Ca, Pb, Mo, Mn, Cr, Co, Ba, As, etc.
    • Pharmaceutical, health, agricultural and environmental and Food Safety.

    Advantages

    Full automation design

    The instrument is thoroughly computer-controlled except for the power switch, which is reliable, safe, and convenient.

    Auto-control of gas flow

    In the sample introduction system, the carrier gas, plasma gas, auxiliary gas are controlled through the advanced mass flow controller (MFC), features continuously adjustable and stable, etc., which ensures the stability of the introduction system and the foundation for the stable light source.

    Peristaltic pump

    A high precision 12 roller, 4 channel peristaltic pump, with speed adjustable according to the demanding, provides smooth, stable sample introduction and drain, to ensure the introduction rate consistent with the drain rate, which is adjusted as per required to stabilize the introduction system.

    Precise wavelength positioning

    Intelligent, precise automatic wavelength calibration algorithm, achieves the measurement without additional peaks calibration, to ensure an accurate measurement whilst saving solution and measurement time.

    advantage of icp oes

    Fast, accurate auto-matching

    The load terminals employs the full-automatic matching technology developed by Drawell, features fast matching, high precision, etc., which could achieve maximum output power, enhance power efficiency, ensure the stability of the instrument whilst facilitating ignition.

    Stable, advanced solid-state RF power

    The instrument employs the solid-state RF power developed by Drwell, which is compact and delivers reliable performance with the power stability and safety, to further improve the instrument’s stability and security.

    Ultra-fast analysis speed

    The analyst can set any suitable integration time for all the analytical lines in one exposure to achieve optimal measurement, or acquire the intensity integral value in the end of the exposure to enable the analysis faster, or specify any one or several specific line(s)to read-out(the readout time<2ms).

    Superb optical system

    Adopting the echelle-prism cross-dispersion type polychromator, elegant optical optimization design maximizes the flux whilst enabling the excellent spectral resolution. No movable optical components achieves unparalleled long-term stability; Ultra-low stray light design with the unique optical design greatly reduces the background interference and further improves the detection limit. A highly efficient N2 distributed purge system for the optical tank combined with the high-quality optics ensures deep UV analysis, especially P, S, As, etc..

    Powerful software analysis function

    Software is easy to operate and intuitive, it offers the capability with qualitative, semi-quantitative and quantitative analysis, instrument diagnostics, intelligent optimization, flexible full-spectrum research function, strong offline reprocessing, scientifically intelligence background correction and interference cancellation algorithm, which enable the analysis more professional and accurate.

    Excellent performance detector

    Employing the CID detector, which is advanced, mature and stable, largest-size active area, megapixel. Full-frame Imaging ability to capture the entire ICP-OES spectrum (165-900 nm) permits quantitative analysis. Non-destructive readout improves the signal-to-noise ratio of weak analyte lines and ensures the precision of results, whist enabling data acquirement and analysis faster than CCD. Excellent linear dynamic range and inherent antiblooming capability allow the measurement of weak analyte emission signals adjacent to intense emission signals, whilst providing flexibility to choose the ideal wavelength for a method (alternative secondary and tertiary lines to overcome interferences).

    Advanced sample introduction system

    The sample introduction system is efficient and stable, equipped with various nebulizers and spray chambers, it can also be equipped with high solids nebulizer, hydrogen fluoride-resistant nebulizer, etc.as per required. Besides, the autosampler developed by Drwell facilitates the operation, and further improves the analysis efficiency.

    Technical parameters

    RF Generator Technical Specifications

    Input Power AC 220V, 20A
    Output power 700-1600W
    Accuracy 2W
    Working Frequency 27.12MHz
    Frequency stability <0.05%
    Output power stability <0.1%
    Match method auto-matching
    Electromagnetic leakage radiation intensity electric field intensity E <0.5V / m at 30cm away from the chamber

    Introduction Sample system Technical Specifications

    Output coil Inner-diameter 25mm, 3 turns
    Quartz tri-concentric torch Outer-diameter 20mm. Various center channel size models optional
    High-efficient nebulizer Concentric nebulizer outer-diameter 6mm. Vvarious models ( high-salt,anti-HF, etc.)optional
    Spray chamber Scott spray chamber, the cyclonic spray chamber with outer diameter 57.2mm optional
    Peristaltic pump 12-roller, 4-channel, the rotation speed can be adjusted according to the demanded flow
    Total consumption(Ar) <14L/min
    Plasma gas flow meter (100-1000)L/h (1.6-16L/min)
    Argon flow meter/carrier Auxiliary gas flow meter(6-60)L/h (0.1-1 L/min)
    Gas pressure gauge Carrier gas flow meter(6-60)L/h (0.1-1 L/min)
    Specifications Carrier gas regulator valve (0.2MPa)
    Cooling water: Water temp. 20-25″C Flow> 5L/min Pressure> 0.1MPa

    Spectrometer Specifications

    Ruled echelle grating 52.67 Ip/mm, 64°blaze angle, the substrate is made of the Zerodur® produced by German SCHOTT, features near-zero thermal expansion coefficient , enabling outstanding performance
    Prism Ultra-pure Corning UV fused silica, transmittance 99.6% at 170nm.
    Wavelength range 175nm-900nm for standard, extended to 165nm-900nm by choosing DUV optical components
    Effective Focal length 430mm
    Numerical aperture F/8, ultra-high flux ensures the instrument detection limit and sensitivity
    Resolution 0.0068nm@200nm
    Stray light Equivalent background concentration of 10000ppmCa solution <2ppm at As189.042nm
    Optical chamber Precisely thermostat, 35±0.1*C
    Distributed N2 purge: normal purge 2L/min, fast purge 4L/min

    Detection Device Technical Specifications

    Detector Type Charge injection detector (CID)
    Pixel Size 27 x27 pm,Random Access Integration (RAI)
    Read mode Full frame readout (FF), Random Access Integration (RAI) with non-destructive read (NDRO)
    Linear dynamic range 108
    Wavelength response range 165nm-1000nm
    Electronic shutter Set the integration time of each line; specify the individual line to read out(read time <2ms)
    Quantum efficiency No coating, up to 35% within 200nm UV region
    Detector cooling High efficiency triple stage thermoelectric cooling device maintains the detector at a constant-45 °C

    Instrument Specifications

    View mode

    Radial view

    Liquid content

    0.01 ppm- several thousands ppm

    Solid content

    0.001%—70%

    Repeatability

    (short-term stability) relative standard deviation RSD <0.5%

    Stability

    Relative standard deviation RSD <1 % within 2 Hours

    Analysis speed

    Single line CID readout time is 2ms, analysis for all elements can be achieved within one minute

    Detection limit (pg/L)

    1 ppb-10ppb for most elements

    Instrument size

    Desktop 1300mm*840mm*740mm

    The typical detection limit of elements

    Element

    Ag

    Ba

    Be

    Ca

    Cr

    Cu

    K

    Li

    Mg

    Wavelength

    328.068

    455.403

    311.107

    393.366

    267.716

    324.754

    766.49

    670.784

    279.553

    Detection limit

    1.31

    0.1

    0.06

    0.02

    1.3

    1.1

    4.9

    0.2

    0.05

    Element

    Mn

    Mo

    Na

    Ni

    Sr

    Ti

    V

    Zn

     

    Wavelength

    257.61

    202.03

    589.592

    231.604

    407.771

    336.121

    309.311

    213.856

     

    Detection limit

    0.22

    1.11

    1.43

    2.19

    0.034

    0.42

    0.88

    0.47

    		  
    Instrument Configuration Working Environment
    Fully automated matcher Manual Store&transport temp.:15°C-25*C Power adaptability:
    The sample introduction system Detection device Store&transport relative humidity:<70% 220±10V,
    Fully automated solid-state RF power Spectrometer Working humidity: <70% 50-60HZ
    Auto-controlled cooling water apparatus Computer system Working temp.: 15，C-30Q  

    Software advantages

    ICP-3000 Software：

    ICP3000 operating software can control all functions of the instrument, including plasma ignition, gas flow control (Figure 1), and security monitoring (Figure 2), etc…

    Figure 1
    Figure 1
    Figure 2
    Figure 2

    Daily Analysis Software：

    specifying the individual pixel or pixel subarray region for quantitative analysis (Figure 3 & 4).

    Figure 3
    Figure 3
    figure 4
    Figure 4

    Methods & data set separation management, strong off-line re-processing function, auto or manual real-time background correction for option(Figure 5)

    Figure 5
    Figure 5

    Fullframe-spectrum mode:

    directly showing the whole emission spectra, directly acquiring the emission intensity, auto-peak identification, interactive spectral library, qualitative&semi-quantitative analysis of the elements (Figures 6, 7 and 8):

    Figure 6
    Figure 6
    Figure 7
    Figure 7
    Figure 8
    Figure 8

    Autosampler mode:the autosampler is provided as per required.

    Calibration type:multi-point calibration curve, of which the number of the standard points is not limited.

    Curve fitting display: linear, auto-adjust the range.

    Data report:export the report based on sample names, method names, elements, intensity, concentration, mean, standard deviation, relative standard deviation, time, date, etc., and generate the analysis report automatically.

    Optional format:analysis data can be stored in user-specified data format, e. g. Excel, Word, PDF, image, etc..

    Instrument structure diagram:

    Instrument structure diagram